1ECE
ACIDOTHERMUS CELLULOLYTICUS ENDOCELLULASE E1 CATALYTIC DOMAIN IN COMPLEX WITH A CELLOTETRAOSE
Experimental procedure
Spacegroup name | P 32 2 1 |
Unit cell lengths | 97.130, 97.130, 258.710 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 10.000 - 2.400 |
R-factor | 0.179 |
Rwork | 0.179 |
R-free | 0.23600 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.200 * |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 9999.000 * |
High resolution limit [Å] | 2.400 |
Rmerge | 0.092 * |
Number of reflections | 47386 |
Completeness [%] | 90.0 |
Redundancy | 2.2 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 4 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | E1cd | 11.4 (mg/ml) | |
2 | 1 | drop | 2.3 (M) | ||
3 | 1 | drop | cellobiose | 0.3 (M) | |
4 | 1 | drop | citrate | 0.1 (M) |