1EAJ
DIMERIC STRUCTURE OF THE COXSACKIE VIRUS AND ADENOVIRUS RECEPTOR D1 DOMAIN AT 1.35 ANGSTROM RESOLUTION
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-2 |
| Synchrotron site | ESRF |
| Beamline | ID14-2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2000-06-01 |
| Detector | ADSC 2X2 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 68.538, 68.538, 146.406 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.000 - 1.350 |
| R-factor | 0.13708 |
| Rwork | 0.137 |
| R-free | 0.14828 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1kac CHAIN B |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | AMoRE |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 1.420 |
| High resolution limit [Å] | 1.350 | 1.350 |
| Rmerge | 0.063 | 0.267 |
| Number of reflections | 73582 | |
| <I/σ(I)> | 5.9 | 2.1 |
| Completeness [%] | 95.1 | 68.7 |
| Redundancy | 4 | 1.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 5.6 | AMMONIUM SULPHATE, SODIUM CITRATE, GLYCEROL, pH 5.60 |
