1E9P
Crystal structure of bovine Cu, Zn SOD to 1.7 Angstrom (3 of 3)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-6A |
Synchrotron site | Photon Factory |
Beamline | BL-6A |
Temperature [K] | 287 |
Detector technology | IMAGE PLATE |
Detector | FUJI |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 47.800, 51.100, 148.000 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 75.000 - 1.700 |
Rwork | 0.185 |
R-free | 0.20200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1cbj |
RMSD bond length | 0.010 |
RMSD bond angle | 0.026 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 75.000 | 1.780 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.065 | 0.300 |
Total number of observations | 104800 * | |
Number of reflections | 40372 * | |
<I/σ(I)> | 9.8 | 2.7 |
Completeness [%] | 91.2 | 91 |
Redundancy | 3 | 2.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 6.5 | 4 * | pH 6.50 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PEG4000 | 17 (%(w/v)) | |
2 | 1 | reservoir | sodium chloride | 100 (mM) |