1E7H
HUMAN SERUM ALBUMIN COMPLEXED WITH HEXADECANOIC ACID (PALMITIC ACID)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X31 |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | X31 |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 1998-10-15 |
Detector | MARRESEARCH |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 190.090, 38.750, 95.870 |
Unit cell angles | 90.00, 104.96, 90.00 |
Refinement procedure
Resolution | 12.000 - 2.430 |
R-factor | 0.214 |
Rwork | 0.214 |
R-free | 0.27200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1bj5 |
RMSD bond length | 0.006 |
RMSD bond angle | 24.600 * |
Data reduction software | MOSFLM |
Data scaling software | CCP4 |
Phasing software | X-PLOR (3.851) |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 11.990 | 2.570 |
High resolution limit [Å] | 2.440 | 2.440 |
Rmerge | 0.046 | 0.178 |
Number of reflections | 24122 | |
<I/σ(I)> | 9.4 | 4 |
Completeness [%] | 92.9 | 87.8 |
Redundancy | 2.7 | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, sitting drop * | 7 | Curry, S., (1998) Nature Struct. Biol., 5, 827. * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 100 (mg/ml) | |
2 | 1 | reservoir | PEG3350 | 25-30 (%(w/v)) | |
3 | 1 | reservoir | potassium phosphate | 50 (mM) |