1E5Z
Azurin from Pseudomonas aeruginosa, reduced form, pH 9.0
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RUH2R |
| Temperature [K] | 288 |
| Detector technology | IMAGE PLATE |
| Collection date | 1991-03-22 |
| Detector | MARRESEARCH |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 57.800, 81.020, 109.990 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 - 2.000 |
| R-factor | 0.19 |
| Rwork | 0.190 |
| Structure solution method | OTHER |
| RMSD bond length | 0.013 |
| RMSD bond angle | 2.900 |
| Data reduction software | MOSFLM |
| Data scaling software | ABSCALE |
| Phasing software | X-PLOR (2.1) |
| Refinement software | X-PLOR (2.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.050 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmerge | 0.075 | |
| Number of reflections | 34847 | |
| Completeness [%] | 90.0 | 83.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 9 | PH 9.0 |
