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1DZH

P14-FLUORESCEIN-N135Q-S380C-ANTITHROMBIN-III

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSRS BEAMLINE PX7.2
Synchrotron siteSRS
BeamlinePX7.2
Temperature [K]100
Detector technologyIMAGE PLATE
DetectorMARRESEARCH
Spacegroup nameP 1 21 1
Unit cell lengths69.175, 99.865, 89.421
Unit cell angles90.00, 105.63, 90.00
Refinement procedure
Resolution20.000 - 2.850
Rwork0.207
R-free0.25800
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2ant
RMSD bond length0.011
RMSD bond angle0.027
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwareAMoRE
Refinement softwareREFMAC
Data quality characteristics
 Overall
Low resolution limit [Å]20.000
High resolution limit [Å]2.850
Rmerge0.073
Total number of observations102580

*

Number of reflections27305
<I/σ(I)>15.5
Completeness [%]99.7
Redundancy3.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1unknown

*

6.55MG/ML 1:1 MIX OF INHIBITORY: LATENT ANTITHROMBIN-III, 10.5% PEG 4000, 65 MM NACACODYLATE, PH 6.5
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
111protein5 (mg/ml)
211PEG400010.5 (%)
311sodium cacodylate65 (mM)

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PDB entries from 2024-10-30

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