1DYM
Humicola insolens Endocellulase Cel7B (EG 1) E197A Mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | X11 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1998-10-15 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 49.969, 74.284, 60.146 |
Unit cell angles | 90.00, 103.82, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.750 |
Rwork | 0.158 |
R-free | 0.20000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2A39 NATIVE STRUCTURE |
RMSD bond length | 0.014 |
RMSD bond angle | 0.031 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.810 |
High resolution limit [Å] | 1.750 | 1.750 |
Rmerge | 0.076 | 0.450 |
Number of reflections | 43135 | |
<I/σ(I)> | 19.7 | 3.3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 4.9 | 4.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8 | 20-30% PEG 4K, 20 MM TRIS-HCL PH 8.0 |