1DXV

HIGH-RESOLUTION X-RAY STUDY OF DEOXY RECOMBINANT HUMAN HEMOGLOBINS SYNTHESIZED FROM BETA-GLOBINS HAVING MUTATED AMINO TERMINI

Experimental procedure

Spacegroup name	P 1 21 1
Unit cell lengths	63.200, 83.600, 53.800
Unit cell angles	90.00, 99.30, 90.00

Refinement procedure

Resolution	6.000 - 1.700
R-factor	0.156
RMSD bond length	0.011
RMSD bond angle	0.025
Refinement software	PROLSQ

Data quality characteristics

	Overall
Low resolution limit [Å]	1.900 *
High resolution limit [Å]	1.750 *
Rmerge	0.037 *
Total number of observations	341064 *
Number of reflections	48575 *
Completeness [%]	85.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Microdialysis *	7 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	2	ammonium phosphate	10 (mM)
2	1	1	hemoglobin