1DXT

HIGH-RESOLUTION X-RAY STUDY OF DEOXY RECOMBINANT HUMAN HEMOGLOBINS SYNTHESIZED FROM BETA-GLOBINS HAVING MUTATED AMINO TERMINI

Experimental procedure

Spacegroup name	P 1 21 1
Unit cell lengths	63.200, 83.600, 53.800
Unit cell angles	90.00, 99.30, 90.00

Refinement procedure

Resolution	6.000 - 1.700
R-factor	0.16
RMSD bond length	0.013
RMSD bond angle	0.029
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	1.800 *
Rmerge	0.034 *
Total number of observations	148393 *
Number of reflections	46131 *
Completeness [%]	90.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Microdialysis *	7 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	2	ammonium phosphate	10 (mM)
2	1	1	hemoglobin