1DWN
Structure of bacteriophage PP7 from Pseudomonas aeruginosa at 3.7 A resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX9.6 |
Synchrotron site | SRS |
Beamline | PX9.6 |
Temperature [K] | 280 |
Collection date | 1998-08-29 |
Spacegroup name | P 1 |
Unit cell lengths | 285.000, 324.000, 380.000 |
Unit cell angles | 88.40, 88.10, 87.70 |
Refinement procedure
Resolution | 60.000 - 3.500 |
R-factor | 0.288 |
Rwork | 0.288 |
R-free | 0.29200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2ms2 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.600 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | RAVE |
Refinement software | CNS (0.5) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 3.490 |
High resolution limit [Å] | 3.400 | 3.400 |
Rmerge | 0.270 | 0.782 * |
Number of reflections | 606783 | |
Completeness [%] | 30.0 | 1.7 |
Redundancy | 1.4 | 1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 5.6 | 310 * | pH 5.60 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | phage | 7 (mg/ml) | |
2 | 1 | reservoir | sodium citrate | 0.1 (M) | |
3 | 1 | reservoir | 1,6-hexanediol | 3.0 (M) |