1DV7

CRYSTAL STRUCTURE OF OROTIDINE MONOPHOSPHATE DECARBOXYLASE

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS
Synchrotron site	APS
Temperature [K]	100
Detector technology	CCD
Collection date	1999-04-24
Detector	ADSC QUANTUM 4
Spacegroup name	P 41 21 2
Unit cell lengths	56.858, 56.858, 124.476
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.000 - 1.800
R-factor	0.2
Rwork	0.200
R-free	0.22200
RMSD bond length	0.012
RMSD bond angle	1.500
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	SOLVE
Refinement software	CNS (0.5)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000	1.860
High resolution limit [Å]	1.800	1.800
Rmerge	0.040	0.076
Total number of observations	153588 *
Number of reflections	20729
Completeness [%]	99.1	99.7
Redundancy	7.4	7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	6.5	298	unpublished data *