Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

1DV6

PHOTOSYNTHETIC REACTION CENTER FROM RHODOBACTER SPHAEROIDES IN THE CHARGE-NEUTRAL DQAQB STATE WITH THE PROTON TRANSFER INHIBITOR ZN2+

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRL BEAMLINE BL9-1
Synchrotron siteSSRL
BeamlineBL9-1
Temperature [K]90
Detector technologyIMAGE PLATE
Collection date1999-05-05
DetectorMARRESEARCH
Spacegroup nameP 43 21 2
Unit cell lengths141.517, 141.517, 278.506
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution27.520 - 2.500
R-factor0.245
Rwork0.238
R-free0.26500
RMSD bond length0.014
RMSD bond angle1.680
Data reduction softwareMOSFLM
Data scaling softwareCCP4 ((SCALA))
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]27.4802.560
High resolution limit [Å]2.5002.500
Rmerge0.0810.307
Total number of observations94697

*

Number of reflections12576

*

<I/σ(I)>7
Completeness [%]96.778.5
Redundancy3.73.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP8

*

25

*

PEG 4000, heptanetriol, TRIS-HCl, LDAO detergent, sodium chloride, pH 8.5, VAPOR DIFFUSION, SITTING DROP, temperature 292K
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropprotein10 (mg/ml)
21dropTris-Cl10 (mM)
31dropPEG40006.0 (%)
41dropampiphiles benzamidine hydrochloride0.4 (%)
51dropheptane triol2.5 (%)
61reservoirPEG400032 (%)

226707

PDB entries from 2024-10-30

PDB statisticsPDBj update infoContact PDBjnumon