1DUZ
HUMAN CLASS I HISTOCOMPATIBILITY ANTIGEN (HLA-A 0201) IN COMPLEX WITH A NONAMERIC PEPTIDE FROM HTLV-1 TAX PROTEIN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | ELLIOTT GX-13 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1996-11-27 |
Detector | MARRESEARCH |
Spacegroup name | P 1 |
Unit cell lengths | 50.560, 63.790, 75.080 |
Unit cell angles | 81.58, 75.66, 77.38 |
Refinement procedure
Resolution | 50.000 - 1.800 |
R-factor | 0.1977 * |
Rwork | 0.198 |
R-free | 0.25020 |
RMSD bond length | 0.030 |
RMSD bond angle | 2.400 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (0.9) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.800 |
Rmerge | 0.042 * |
Total number of observations | 137168 * |
Number of reflections | 72184 * |
Completeness [%] | 85.3 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | 13-20% polyethylene glycol 6000, 25 mM MES buffer, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 5 (mg/ml) | |
2 | 1 | drop | MES | 25 (mM) | |
3 | 1 | reservoir | PEG6000 | 13-20 (%) | |
4 | 1 | reservoir | MES | 25 (mM) |