1DUK
WILD-TYPE RECOMBINANT SPERM WHALE METAQUOMYOGLOBIN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Detector technology | AREA DETECTOR |
Collection date | 1994-02-11 |
Detector | SDMS |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 40.132, 49.071, 79.339 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.130 |
R-factor | 0.18 |
RMSD bond length | 0.020 |
RMSD bond angle | 3.000 |
Data reduction software | SDMS |
Data scaling software | SDMS |
Phasing software | TNT |
Refinement software | TNT |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.290 |
High resolution limit [Å] | 2.130 | 2.130 |
Rmerge | 0.053 | 0.163 |
Number of reflections | 7405 | |
<I/σ(I)> | 7.74 | |
Completeness [%] | 78.0 | 47 |
Redundancy | 2.21 | 1.36 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 * | drop consists of equal volume of protein and reservoir solutions * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | Mb solution | 1 (%) | |
2 | 1 | reservoir | PEG8000 | 35-37.5 (%) | |
3 | 1 | reservoir | 0.3-0.35 (M) | ||
4 | 1 | reservoir | PIPES | 0.1 (M) | |
5 | 1 | reservoir | dioxane | 0.1 (%) |