1DUD
DEOXYURIDINE 5'-TRIPHOSPHATE NUCLEOTIDE HYDROLASE (D-UTPASE) COMPLEXED WITH THE SUBSTRATE ANALOGUE DEOXYURIDINE 5'-DIPHOSPHATE (D-UDP)
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RUH2R |
Detector technology | AREA DETECTOR |
Detector | SIEMENS |
Spacegroup name | H 3 |
Unit cell lengths | 86.640, 86.640, 62.230 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 10.000 - 2.300 |
R-factor | 0.2 |
Rwork | 0.200 |
RMSD bond length | 0.017 |
RMSD bond angle | 27.900 * |
Data reduction software | XDS |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 4.480 * | |
High resolution limit [Å] | 2.250 | 2.250 * |
Rmerge | 0.072 | 0.304 * |
Total number of observations | 33369 * | |
Number of reflections | 7520 | |
Completeness [%] | 67.0 | 35 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Batch method * | 4.5 * | 20 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | enzyme | 3.4 (mg/ml) | |
2 | 1 | 1 | succinate | 7 (mM) | |
3 | 1 | 1 | PEG8000 | 1.5 (%) |