1DTN
MANDELATE RACEMASE MUTANT D270N CO-CRYSTALLIZED WITH (S)-ATROLACTATE
Experimental procedure
Detector technology | AREA DETECTOR |
Collection date | 1992-06-03 |
Detector | SIEMENS |
Spacegroup name | I 4 2 2 |
Unit cell lengths | 125.500, 125.500, 107.300 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.100 |
R-factor | 0.171 * |
Rwork | 0.171 |
RMSD bond length | 0.010 |
RMSD bond angle | 2.200 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | X-PLOR |
Refinement software | TNT |
Data quality characteristics
Overall | |
Rmerge | 0.130 |
Number of reflections | 24924 |
Completeness [%] | 85.3 |
Redundancy | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 7.5 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | Tris | 50 (mM) | |
2 | 1 | drop | 10 (mM) | ||
3 | 1 | drop | (S)-atrolactate | 50 (mM) | |
4 | 1 | drop | E317Q | 13 (mg/ml) | |
5 | 1 | drop | atrolactate | 5 (mM) | |
6 | 1 | reservoir | 30 (%) | ||
7 | 1 | reservoir | acetone | 3 (%(v/v)) |