1DTM
CRYSTAL STRUCTURE OF THE SPERM-WHALE MYOGLOBIN MUTANT H93G COMPLEXED WITH 4-METHYLIMIDAZOLE, METAQUO FORM
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 298 |
Detector technology | AREA DETECTOR |
Collection date | 1994-07-29 |
Detector | SDMS |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 40.276, 48.892, 78.935 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.130 |
R-factor | 0.175 |
RMSD bond length | 0.019 |
RMSD bond angle | 2.900 |
Data reduction software | SDMS |
Data scaling software | SDMS |
Phasing software | TNT |
Refinement software | TNT |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.298 |
High resolution limit [Å] | 2.130 | 2.130 |
Rmerge | 0.036 | 0.141 |
Number of reflections | 7356 | |
<I/σ(I)> | 12.54 | |
Completeness [%] | 78.9 | 49 |
Redundancy | 2.63 | 1.51 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | drop consists of equal volume of protein and reservoir solutions * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | Mb solution | 1 (%) | |
2 | 1 | reservoir | PEG8000 | 35-37.5 (%) | |
3 | 1 | reservoir | 0.3-0.35 (M) | ||
4 | 1 | reservoir | PIPES | 0.1 (M) | |
5 | 1 | reservoir | dioxane | 0.1 (%) |