1DSL

GAMMA B CRYSTALLIN C-TERMINAL DOMAIN

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	33.450, 50.080, 53.110
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 1.550
R-factor	0.21
Rwork	0.210
RMSD bond length	0.017
RMSD bond angle	3.020
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000
High resolution limit [Å]	1.550
Rmerge	0.055
Total number of observations	69882 *
Number of reflections	12582 *
Completeness [%]	94.2
Redundancy	5.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *		19 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	gammaB-C	0.8 (mg/ml)
2	1	drop		0.1 (M)
3	1	reservoir		0.4 (M)