1DRG
CRYSTAL STRUCTURE OF TRIMERIC CRE RECOMBINASE-LOX COMPLEX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1998-01-01 |
Detector | RIGAKU RAXIS IV |
Spacegroup name | I 2 3 |
Unit cell lengths | 160.990, 160.990, 160.990 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 5.000 - 2.550 |
R-factor | 0.186 * |
Rwork | 0.186 |
R-free | 0.26800 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.280 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MLPHARE |
Refinement software | TNT (5E) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 81.000 | 2.640 |
High resolution limit [Å] | 2.550 | 2.550 |
Rmerge | 0.062 | 0.298 |
Number of reflections | 22679 | |
<I/σ(I)> | 7.1 | |
Completeness [%] | 99.7 | 100 |
Redundancy | 5.2 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 6.1 | 20-22 * | 125 MM LI2SO4, 4% PEG 8000, 40MM NAPIPES PH 6.1, VAPOR DIFFUSION, HANGING DROP AT 293K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | LI2SO4 | ||
2 | 1 | 1 | NAPIPES | ||
3 | 1 | 1 | PEG 8000 | ||
4 | 1 | 2 | PEG 8000 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PEG8000 | 4 (%(w/v)) | |
2 | 1 | reservoir | 125 (mM) | ||
3 | 1 | reservoir | 20 (mM) | ||
4 | 1 | reservoir | 60 (mM) |