1DNH
THE MOLECULAR STRUCTURE OF THE COMPLEX OF HOECHST 33258 AND THE DNA DODECAMER D(CGCGAATTCGCG)
Experimental procedure
Temperature [K] | 288 |
Detector technology | DIFFRACTOMETER |
Detector | NICOLET P3 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 25.230, 40.580, 66.080 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.250 |
R-factor | 0.157 |
Refinement software | NUCLSQ |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.250 |
Number of reflections | 3634 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.5 * | VAPOR DIFFUSION |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | MPD | ||
3 | 1 | 1 | NA CACODYLATE | ||
4 | 1 | 1 | SPERMINE | ||
5 | 1 | 2 | WATER | ||
6 | 1 | 2 | MPD |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | DNA dodecamer | 1.2 (mM) | single strand |
2 | 1 | drop | sodium cacodylate | 20 (mM) | |
3 | 1 | drop | (mM) | ||
4 | 1 | drop | spermine tetrachloride | 1 (mM) | |
5 | 1 | drop | Hoechst 33258 | 1.2 (mM) | |
6 | 1 | drop | 12 (%) | ||
7 | 1 | reservoir | MPD | 50 (%) |