1DN5
SOLVATION OF THE LEFT-HANDED HEXAMER D(5BRC-G-5BRC-G-5BRC-G) IN CRYSTALS GROWN AT TWO TEMPERATURES
Experimental procedure
Temperature [K] | 310 |
Detector technology | DIFFRACTOMETER |
Detector | ENRAF-NONIUS CAD4 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 17.930, 30.830, 44.730 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.400 |
R-factor | 0.1247 |
Refinement software | NUCLSQ |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 10.000 |
High resolution limit [Å] | 1.400 |
Number of reflections | 3765 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.5 * | 37 * | VAPOR DIFFUSION, temperature 310.00K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | MPD | ||
3 | 1 | 1 | NA CACODYLATE | ||
4 | 1 | 1 | NACL | ||
5 | 1 | 2 | WATER | ||
6 | 1 | 2 | MPD |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | sodium cacodylate | 20 (mM) | |
2 | 1 | drop | 200 (mM) | ||
3 | 1 | drop | protein | 1 (mg/ml) | |
4 | 1 | reservoir | MPD | 10-60 (%) |