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1DMS

STRUCTURE OF DMSO REDUCTASE

Experimental procedure
Source typeSYNCHROTRON
Source detailsMPG/DESY, HAMBURG BEAMLINE BW6
Synchrotron siteMPG/DESY, HAMBURG
BeamlineBW6
Temperature [K]289
Detector technologyIMAGE PLATE
Collection date1994-06-17
DetectorMARRESEARCH
Wavelength(s)1.0
Spacegroup nameP 41 21 2
Unit cell lengths80.700, 80.700, 229.200
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution8.000 - 1.880
R-factor0.169
Rwork0.169
R-free0.20300
RMSD bond length0.009

*

RMSD bond angle1.775

*

Data reduction softwareMOSFLM (V. 5.21-5.23)
Phasing softwareX-PLOR (3.1)
Refinement softwareX-PLOR (3.1)
Data quality characteristics
 Overall
High resolution limit [Å]1.880

*

Rmerge0.059
Total number of observations227189

*

Number of reflections58291

*

Completeness [%]93.3
Redundancy3.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Vapor diffusion

*

6.5

*

30

*

Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropMPD30 (%(v/v))
21dropPEG400010 (%(w/v))
31reservoirMES0.1 (M)

217705

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