1DMA
DOMAIN III OF PSEUDOMONAS AERUGINOSA EXOTOXIN COMPLEXED WITH NICOTINAMIDE AND AMP
Experimental procedure
Spacegroup name | P 43 21 2 |
Unit cell lengths | 87.510, 87.510, 134.080 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.500 |
R-factor | 0.195 |
Rwork | 0.195 |
R-free | 0.26400 * |
RMSD bond length | 0.019 |
RMSD bond angle | 26.200 * |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 8.000 |
High resolution limit [Å] | 2.500 |
Rmerge | 0.068 * |
Number of reflections | 16513 |
Completeness [%] | 88.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 7 * | used as seeds * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | sodium citrate | 1.5 (M) | |
2 | 1 | reservoir | NAD | 40 (mM) | |
3 | 1 | drop | PEIII | 10 (mg/ml) | |
4 | 1 | drop | Tris-HCl | 10 (mM) | |
5 | 1 | drop | 0.1 (M) | ||
6 | 1 | drop | sodium citrate | 1.5 (M) | |
7 | 1 | drop | NAD | 40 (mM) |