1DLC

CRYSTAL STRUCTURE OF INSECTICIDAL DELTA-ENDOTOXIN FROM BACILLUS THURINGIENSIS AT 2.5 ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	C 2 2 21
Unit cell lengths	117.090, 134.260, 104.500
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	16.000 - 2.500
R-factor	0.183
Rwork	0.183
RMSD bond length	0.011
RMSD bond angle	1.580
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.500 *
Rmerge	0.108 *
Total number of observations	121767 *
Number of reflections	27727 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Microdialysis *	9.5 *	4 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	protein	2.5 (mg/ml)
2	1	2		0.1 (M)
3	1	2		1.2 (M)