1DKJ

BOBWHITE QUAIL LYSOZYME

Experimental procedure

Detector technology	AREA DETECTOR
Collection date	1992-02
Detector	SIEMENS-NICOLET X100
Spacegroup name	P 61 2 2
Unit cell lengths	89.200, 89.200, 61.700
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	6.000 - 2.000
R-factor	0.177 *
Rwork	0.177
RMSD bond length	0.012
RMSD bond angle	24.000 *
Data reduction software	XENGEN
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.000 *
Rmerge	0.057
Total number of observations	49907 *
Number of reflections	9288 *
Completeness [%]	92.9 *
Redundancy	5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	4 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	sodium acetate	5 (mM)
2	1	drop	BWQL	45 (mg/ml)
3	1	drop	formamide	0.625 (mM)
4	1	drop	sodium nitrate	6 (%(w/v))
5	1	reservoir	sodium acetate	10 (mM)
6	1	reservoir	formamide	1.25 (mM)
7	1	reservoir	sodium nitrate	12 (%(w/v))