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1DIK

PYRUVATE PHOSPHATE DIKINASE

Experimental procedure
Source typeROTATING ANODE
Source detailsRIGAKU RU200
Temperature [K]295
Detector technologyAREA DETECTOR
Collection date1991-01-07
DetectorSIEMENS
Spacegroup nameP 1 2 1
Unit cell lengths89.800, 58.800, 102.000
Unit cell angles90.00, 94.80, 90.00
Refinement procedure
Resolution8.000 - 2.300
R-factor0.182
Rwork0.182
RMSD bond length0.019
RMSD bond angle2.100
Data reduction softwareXENGEN
Phasing softwareX-PLOR
Refinement softwareX-PLOR
Data quality characteristics
 Overall
Low resolution limit [Å]28.300
High resolution limit [Å]2.300
Rmerge0.082
Number of reflections44378
Completeness [%]93.0
Redundancy2.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Vapor diffusion, hanging drop

*

730

*

pH 7.0
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropprotein10 (mg/ml)
21dropimidazole20 (mM)
31drop100 (mM)
41dropEDTA0.1 (mM)
51drop2-mercaptoethanol1 (mM)
61reservoirammonium sulfate50-55 (%sat)

227561

PDB entries from 2024-11-20

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