1DDL
DESMODIUM YELLOW MOTTLE TYMOVIRUS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL7-1 |
Synchrotron site | SSRL |
Beamline | BL7-1 |
Temperature [K] | 295 |
Detector technology | IMAGE PLATE |
Collection date | 1996-03-28 |
Detector | MARRESEARCH |
Spacegroup name | P 42 3 2 |
Unit cell lengths | 348.546, 348.546, 348.546 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.000 - 2.700 |
R-factor | 0.152 |
Rwork | 0.151 |
R-free | 0.15900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | TURNIP YELLOW MOSAIC VIRUS |
RMSD bond length | 0.010 |
RMSD bond angle | 1.900 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.800 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.107 | 0.453 |
Total number of observations | 574527 * | |
Number of reflections | 178705 | |
<I/σ(I)> | 7.3 | |
Completeness [%] | 91.3 * | 82.7 |
Redundancy | 3.2 | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, sitting drop * | 4.8 | 295 | 2 M SODIUM FORMATE, 0.1 M SODIUM ACETATE, POTASSIUM PHOSPHATE BUFFER, pH 4.8, VAPOR DIFFUSION, BOTH SITTING DROP AND HANGING DROP, temperature 295K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | SODIUM FORMATE | ||
2 | 1 | 1 | SODIUM ACETATE | ||
3 | 1 | 1 | POTASSIUM PHOSPHATE BUFFER | ||
4 | 1 | 2 | SODIUM FORMATE | ||
5 | 1 | 2 | SODIUM ACETATE | ||
6 | 1 | 2 | POTASSIUM PHOSPHATE BUFFER |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 3 (mg/ml) | |
2 | 1 | reservoir | sodium formate | 2.0-2.2 (M) | |
3 | 1 | reservoir | sodium acetate | 0.1 (M) |