1DCC

2.2 ANGSTROM STRUCTURE OF OXYPEROXIDASE: A MODEL FOR THE ENZYME:PEROXIDE COMPLEX

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	104.722, 74.446, 45.170
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	? - 2.200
R-factor	0.155
RMSD bond length	0.007
RMSD bond angle	2.500
Refinement software	TNT

Data quality characteristics

	Overall
High resolution limit [Å]	2.200 *
Total number of observations	16002 *
Completeness [%]	87.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, sitting drop *	6 *	4 *	referred to Biochemistry 29.7160-7173 1990 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	10 (mg/ml)
2	1	drop	potassium phosphate	0.10 (M)
3	1	drop	MPD/water	40 (%(v/v))
4	1	reservoir	MPD/water	30 (%(v/v))