1DAH
DETHIOBIOTIN SYNTHETASE COMPLEXED WITH 7,8-DIAMINO-NONANOIC ACID, 5'-ADENOSYL-METHYLENE-TRIPHOSPHATE, AND MANGANESE
Experimental procedure
Detector technology | IMAGE PLATE |
Collection date | 1994-02-15 |
Detector | RIGAKU RAXIS II |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 73.200, 49.200, 61.800 |
Unit cell angles | 90.00, 107.10, 90.00 |
Refinement procedure
Resolution | 6.000 - 1.640 |
R-factor | 0.174 |
Rwork | 0.174 |
RMSD bond length | 0.013 |
RMSD bond angle | 24.600 * |
Data reduction software | R-AXIS |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.640 * |
Rmerge | 0.079 |
Total number of observations | 38766 * |
Number of reflections | 19323 |
Completeness [%] | 75.0 |
Redundancy | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | other * | cocrystallization * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | AMPPCP | 5 (mM) | |
2 | 1 | 1 | 200 (mM) | or 100mM MnCl2 |