1DA0
DNA-DRUG INTERACTIONS: THE CRYSTAL STRUCTURE OF D(CGATCG) COMPLEXED WITH DAUNOMYCIN
Experimental procedure
Temperature [K] | 277 |
Detector technology | DIFFRACTOMETER |
Detector | SYNTEX P21 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 27.980, 27.980, 52.870 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.500 |
R-factor | 0.25 |
Refinement software | NUCLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.500 |
Rmerge | 0.090 |
Number of reflections | 2801 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.5 | 20 * | pH 6.50, VAPOR DIFFUSION, temperature 293.00K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | MPD | ||
3 | 1 | 1 | MG ACETATE | ||
4 | 1 | 1 | SPERMINE_HCL | ||
5 | 1 | 1 | NA CACODYLATE | ||
6 | 1 | 2 | WATER | ||
7 | 1 | 2 | MPD |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | d(CGATCG) | 1.5 (mM) | single stranded |
2 | 1 | drop | daunomycin hydrochloride | 1.5 (mM) | |
3 | 1 | drop | magnesium acetate | 20 (mM) | |
4 | 1 | drop | spermine hydrochloride | 3.5 (mM) | |
5 | 1 | drop | sodium cacodylate | 20 (mM) | |
6 | 1 | drop | MPD | 9 (%(v/v)) | |
7 | 1 | reservoir | 50 (%(v/v)) |