1D92
REFINED CRYSTAL STRUCTURE OF AN OCTANUCLEOTIDE DUPLEX WITH G.T MISMATCHED BASE-PAIRS
Experimental procedure
Temperature [K] | 275 |
Detector technology | DIFFRACTOMETER |
Detector | SYNTEX P21 |
Spacegroup name | P 61 |
Unit cell lengths | 45.200, 45.200, 42.970 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 10.000 - 2.250 |
R-factor | 0.136 |
RMSD bond length | 0.026 * |
RMSD bond angle | 0.041 * |
Refinement software | NUCLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.250 |
Rmerge | 0.060 * |
Number of reflections | 2414 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | other * | 6.5 | 4 * | pH 6.50, VAPOR DIFFUSION, temperature 277.00K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | NA CACODYLATE | ||
3 | 1 | 1 | MGCL2 | ||
4 | 1 | 2 | WATER |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | sodium cacodylate | 3 (mM) |