1D8A

E. COLI ENOYL REDUCTASE/NAD+/TRICLOSAN COMPLEX

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SRS BEAMLINE PX7.2
Synchrotron site	SRS
Beamline	PX7.2
Temperature [K]	298
Detector technology	IMAGE PLATE
Collection date	1998-09-25
Detector	MARRESEARCH
Spacegroup name	P 61 2 2
Unit cell lengths	80.600, 80.600, 327.600
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	20.000 - 2.200
R-free	0.29400
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	TNT
Refinement software	TNT

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	999.000	2.240
High resolution limit [Å]	2.200	2.180
Rmerge	0.057
Number of reflections	153843
Completeness [%]	78.0

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	7.5	290	This particular structure is not described in this paper. *