1D89
A DNA DODECAMER CONTAINING AN ADENINE TRACT CRYSTALLIZES IN A UNIQUE LATTICE AND EXHIBITS A NEW BEND
Experimental procedure
Temperature [K] | 263 |
Detector technology | AREA DETECTOR |
Detector | UCSD MARK II |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 44.780, 66.050, 42.910 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 - 2.300 |
R-factor | 0.232 |
Rwork | 0.232 |
RMSD bond length | 0.012 |
RMSD bond angle | 3.200 |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.300 |
Rmerge | 0.051 * |
Total number of observations | 24066 * |
Number of reflections | 5545 |
Completeness [%] | 92.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 10 * | pH 7.00, VAPOR DIFFUSION, SITTING DROP, temperature 283.00K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | MPD | ||
3 | 1 | 1 | MGCL2 | ||
4 | 1 | 1 | NA CACODYLATE | ||
5 | 1 | 1 | SPERMINE | ||
6 | 1 | 2 | WATER | ||
7 | 1 | 2 | MPD |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | duplex | 5 (mg/ml) | |
2 | 1 | reservoir | 93 (mM) | ||
3 | 1 | reservoir | sodium cacodylate | 10 (mM) | |
4 | 1 | reservoir | spermine tetrahydrochloride | 1 (mM) | |
5 | 1 | reservoir | MPD | 31 (%) |