1D82
CRYSTAL AND MOLECULAR STRUCTURE OF D(GTCTAGAC)
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 295 |
Detector technology | DIFFRACTOMETER |
Detector | RIGAKU AFC-5 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 42.560, 42.560, 24.610 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 - 2.500 |
R-factor | 0.211 |
Refinement software | NUCLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.500 |
Number of reflections | 1757 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, sitting drop * | 6.8 | 295 | pH 6.80, VAPOR DIFFUSION, temperature 295.00K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | MPD | ||
3 | 1 | 1 | NA CACODYLATE | ||
4 | 1 | 1 | MGCL2 | ||
5 | 1 | 1 | SPERMINE_HCL | ||
6 | 1 | 2 | WATER | ||
7 | 1 | 2 | MPD |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | DNA | 6 (mg/ml) | |
2 | 1 | drop | sodium cacodylate | 60 (mM) | |
3 | 1 | drop | magnesium cacodylate | 25 (mM) | |
4 | 1 | drop | spermine tetrachloride | 6 (mM) | |
5 | 1 | drop | MPD | 10 (%(v/v)) | |
6 | 1 | reservoir | MPD | 50 (%) |