1D81
THE CONFORMATIONAL VARIABILITY OF AN ADENOSINE. INOSINE BASE-PAIR IN A SYNTHETIC DNA DODECAMER
Experimental procedure
Temperature [K] | 277 |
Detector technology | DIFFRACTOMETER |
Detector | SIEMENS AED2 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 25.160, 41.060, 65.450 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 7.000 - 2.500 |
R-factor | 0.158 |
RMSD bond length | 0.011 |
RMSD bond angle | 0.025 |
Refinement software | NUCLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.500 |
Rmerge | 0.090 |
Number of reflections | 2462 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 4 * | pH 6.50, VAPOR DIFFUSION, SITTING DROP, temperature 277.00K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | MPD | ||
3 | 1 | 1 | NA CACODYLATE | ||
4 | 1 | 1 | SPERMINE_HCL | ||
5 | 1 | 2 | WATER | ||
6 | 1 | 2 | MPD |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 0.5 (mM) | |
2 | 1 | drop | sodium cacodylate | 15 (mM) | |
3 | 1 | drop | magnesium chloride | 40 (mM) | |
4 | 1 | drop | spermine-HCl | 0.3 (mM) | |
5 | 1 | drop | MPD | (%(v/v)) | |
6 | 1 | reservoir | 50 (%(v/v)) |