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1D7H

FKBP COMPLEXED WITH DMSO

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsENRAF-NONIUS FR571
Temperature [K]297
Detector technologyAREA DETECTOR
Collection date1995-01-01
DetectorENRAF-NONIUS
Spacegroup nameC 1 2 1
Unit cell lengths102.800, 36.450, 56.000
Unit cell angles90.00, 96.00, 90.00
Refinement procedure
Resolution20.000 - 1.900
R-factor0.213
Rwork0.213
R-free0.27300
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.009
RMSD bond angle27.221

*

Data reduction softwareMADNESS
Data scaling softwareCCP4 ((AGROVATA)
Phasing softwareX-PLOR
Refinement softwareX-PLOR (3.1)
Data quality characteristics
 Overall
Low resolution limit [Å]100.000
High resolution limit [Å]1.900
Rmerge0.070
Number of reflections14868
Completeness [%]97.0
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP829756 % SAT. AMMONIUM SULFATE 5 % DMSO, 100 MM TRIS (PH 8.0), VAPOR DIFFUSION, HANGING DROP, temperature 297K
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropprotein0.6 (mM)
21dropDMSO340 (mM)
31dropTris-HCl50 (mM)
41dropammonium sulfate28 (%(w/v))
51reservoirammonium sulfate
61reservoirDMSO
71reservoirTris-HCl1 (M)

222036

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