1D2Q
CRYSTAL STRUCTURE OF HUMAN TRAIL
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | MACSCIENCE |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | MACSCIENCE |
Spacegroup name | P 63 |
Unit cell lengths | 65.610, 65.610, 131.700 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | ? - 2.800 |
Rwork | 0.209 |
R-free | 0.28200 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.662 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.063 | |
Completeness [%] | 89.6 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 9 | 295 | PEG 550 MME, bicine pH 9.0, cadmium chloride, EVAPORATION, temperature 22K |
1 | unknown * | 9 | 295 | PEG 550 MME, bicine pH 9.0, cadmium chloride, EVAPORATION, temperature 22K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | mPEG550 | 25 (%) | |
2 | 1 | 1 | bicine | 0.05 (M) | |
3 | 1 | 1 | 10 (mM) |