1D22
BINDING OF THE ANTITUMOR DRUG NOGALAMYCIN AND ITS DERIVATIVES TO DNA: STRUCTURAL COMPARISON
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 298 |
Detector technology | DIFFRACTOMETER |
Detector | RIGAKU AFC-5R |
Spacegroup name | P 61 |
Unit cell lengths | 26.270, 26.270, 100.230 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | ? - 1.800 |
R-factor | 0.196 |
RMSD bond length | 0.025 |
RMSD bond angle | 0.040 |
Refinement software | NUCLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.800 |
Number of reflections | 2143 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 5 | 25 * | pH 5.00, VAPOR DIFFUSION, temperature 298.00K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | PEG 400 | ||
3 | 1 | 1 | MGCL2 | ||
4 | 1 | 1 | NA CACODYLATE | ||
5 | 1 | 2 | WATER | ||
6 | 1 | 2 | PEG 400 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | oligonucleotide | 0.5 (mM) | |
2 | 1 | drop | 8 (mM) | ||
3 | 1 | drop | sodium cacodylate | 30 (mM) | |
4 | 1 | drop | nogalamycin | 0.5 (mM) | |
5 | 1 | drop | PEG400 | 2 (%(w/v)) | |
6 | 1 | reservoir | PEG400 | 30 (%) |