1D13
MOLECULAR STRUCTURE OF AN A-DNA DECAMER D(ACCGGCCGGT)
Experimental procedure
| Temperature [K] | 283 |
| Detector technology | DIFFRACTOMETER |
| Detector | NICOLET P3 |
| Spacegroup name | P 61 2 2 |
| Unit cell lengths | 39.230, 39.230, 78.010 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 20.000 - 2.000 |
| R-factor | 0.18 |
| RMSD bond length | 0.026 |
| Refinement software | NUCLSQ |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.000 |
| Number of reflections | 1434 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 6.5 * | VAPOR DIFFUSION |
Crystallization Reagents
| ID | crystal ID | solution ID | reagent name | concentration | details |
| 1 | 1 | 1 | WATER | ||
| 2 | 1 | 1 | MPD | ||
| 3 | 1 | 1 | NA CACODYLATE | ||
| 4 | 1 | 1 | MGCL2 | ||
| 5 | 1 | 1 | SPERMINE |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | DNA decamer | 1 (mM) | single strand |
| 2 | 1 | drop | sodium cacodylate | 40 (mM) | |
| 3 | 1 | drop | magnesium chloride | 13.0 (mM) | |
| 4 | 1 | drop | spermine tetrachloride | 5.0 (mM) | |
| 5 | 1 | drop | MPD | 5 (%) | |
| 6 | 1 | reservoir | MPD | 50 (%) |
