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1D0H

THE HC FRAGMENT OF TETANUS TOXIN COMPLEXED WITH N-ACETYL-GALACTOSAMINE

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSRS BEAMLINE PX9.6
Synchrotron siteSRS
BeamlinePX9.6
Temperature [K]100
Detector technologyCCD
Collection date1998-09-16
DetectorADSC QUANTUM 4
Spacegroup nameP 21 21 21
Unit cell lengths67.076, 70.882, 122.238
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution40.000 - 2.100
R-factor0.204

*

Rwork0.204
R-free0.27000
Structure solution methodPHASES FROM ISOMORPHOUS STRUCTURE, THE HC-LACTOSE COMPLEX
RMSD bond length0.010
RMSD bond angle0.031
Data scaling softwareCCP4 ((SCALA))
Refinement softwareREFMAC
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]40.0002.190
High resolution limit [Å]2.1002.100
Rmerge0.1360.665
Total number of observations238621

*

Number of reflections34754
<I/σ(I)>4.6
Completeness [%]99.999.8
Redundancy6.65.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Vapor diffusion, sitting drop

*

7pH 7.00
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropprotein3 (mg/ml)
21dropimidazole20 (mM)
31drop100 (mM)
41reservoirammonium sulfate200 (mM)
51reservoirPEG400040 (%(w/v))
61reservoirMPD1 (%(v/v))

217705

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