1CZW
STRUCTURE OF THE W34A MUTANT OF SHIGA-LIKE TOXIN I B SUBUNIT
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | SIEMENS |
Temperature [K] | 298 |
Detector technology | AREA DETECTOR |
Collection date | 1995-04-22 |
Detector | SIEMENS |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 107.550, 108.920, 57.350 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.600 - 2.500 |
R-factor | 0.182 |
Rwork | 0.182 |
R-free | 0.21400 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.967 |
Data reduction software | X-GEN |
Data scaling software | X-GEN |
Phasing software | AMoRE |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.600 | 2.540 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.127 | 0.365 |
Number of reflections | 23240 | |
<I/σ(I)> | 11.5 | |
Completeness [%] | 96.8 | 53.3 |
Redundancy | 6.7 | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 298 | 15% PEG 4000 0.2 M MGCL2 5% DIOXANE, pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 298.0K |