Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 64.540, 46.040, 29.910 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.500 |
R-factor | 0.16 |
Rwork | 0.160 |
RMSD bond length | 0.009 * |
RMSD bond angle | 1.200 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 2.200 * | |
High resolution limit [Å] | 1.500 * | 1.500 * |
Total number of observations | 13356 * | |
Number of reflections | 9843 * | |
Completeness [%] | 99.2 * | 16.5 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 3 (mg/ml) | |
2 | 1 | drop | phosphate | 2.6 (M) | |
3 | 1 | reservoir | phosphate | 3.2 (M) |