1CUK

ESCHERICHIA COLI RUVA PROTEIN AT PH 4.9 AND ROOM TEMPERATURE

Experimental procedure

Detector technology	AREA DETECTOR
Collection date	1995-10-26
Detector	XUONG-HAMLIN MULTIWIRE
Spacegroup name	P 4
Unit cell lengths	83.700, 83.700, 33.100
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	15.000 - 1.900
Rwork	0.209
R-free	0.02700 *
RMSD bond length	0.016
RMSD bond angle	1.900
Data reduction software	SDMS
Refinement software	TNT

Data quality characteristics

	Overall
Rmerge	0.073
Number of reflections	16391
Completeness [%]	89.0
Redundancy	2.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *			Sedelnikova, S.E., (1999) Acta Crystallogr. D., 55, 263. *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	9 (mg/ml)
2	1	drop	imidazole-HCl	0.1 (M)
3	1	reservoir	sodium acetate	0.70-0.95 (M)