1CUH
CUTINASE, R196E MUTANT
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RUH2R |
Temperature [K] | 293 |
Detector technology | IMAGE PLATE |
Detector | MAR scanner 180 mm plate |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 37.000, 64.200, 71.400 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 - 1.750 |
R-factor | 0.163 |
Rwork | 0.163 |
RMSD bond length | 0.012 |
RMSD bond angle | 2.500 |
Data reduction software | MARXDS |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.750 * |
Rmerge | 0.067 |
Total number of observations | 75375 * |
Number of reflections | 16320 |
Completeness [%] | 92.0 |
Redundancy | 4.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | PEG6000 | 2-20 (%(w/v)) | |
2 | 1 | drop | HEPES | 100 (mM) | |
3 | 1 | drop | cutinase | 5-15 (mg/ml) |