1CSK

THE CRYSTAL STRUCTURE OF HUMAN CSKSH3: STRUCTURAL DIVERSITY NEAR THE RT-SRC AND N-SRC LOOP

Experimental procedure

Spacegroup name	C 2 2 21
Unit cell lengths	64.900, 74.690, 125.030
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 2.500
R-factor	0.224
Rwork	0.224
R-free	0.27800
RMSD bond length	0.013
RMSD bond angle	1.900
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	25.000 *
High resolution limit [Å]	2.500 *
Rmerge	0.083 *
Total number of observations	60252 *
Number of reflections	10807 *
Completeness [%]	94.8 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	2	TEA/HCl	10 (mM)
2	1	2		20 (mM)
3	1	2	DTT	1 (mM)
4	1	2	EDTA	1 (mM)
5	1	2		1 (mM)
6	1	1	protein	10 (mg/ml)