1CRJ
THE ROLE OF A CONSERVED INTERNAL WATER MOLECULE AND ITS ASSOCIATED HYDROGEN BOND NETWORK IN CYTOCHROME C
Experimental procedure
Spacegroup name | P 43 21 2 |
Unit cell lengths | 36.560, 36.560, 137.530 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | ? - 2.050 |
R-factor | 0.179 |
RMSD bond length | 0.022 |
RMSD bond angle | 0.044 * |
Refinement software | PROLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.050 * |
Rmerge | 0.070 * |
Total number of observations | 33491 * |
Number of reflections | 5700 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | using a hair-seeding * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | sodium phosphate | 0.1 (M) | |
2 | 1 | reservoir | ammonium sulphate | 86-94 (%sat) | |
3 | 1 | drop | DTT | 20 (mM) | can be replaced with 70mM sodium dithionite |