1CPR
ST. LOUIS CYTOCHROME C' FROM THE PURPLE PHOTOTROPIC BACTERIUM, RHODOBACTER CAPSULATUS
Experimental procedure
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-6A |
Synchrotron site | Photon Factory |
Beamline | BL-6A |
Detector technology | IMAGE PLATE |
Collection date | 1995-12-19 |
Detector | FUJI |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 39.680, 46.850, 40.750 |
Unit cell angles | 90.00, 110.94, 90.00 |
Refinement procedure
Resolution | 6.000 - 2.100 |
R-factor | 0.184 |
Rwork | 0.184 |
RMSD bond length | 0.009 |
RMSD bond angle | 20.020 * |
Data reduction software | DENZO |
Phasing software | X-PLOR (2.1) |
Refinement software | X-PLOR (2.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 * | |
High resolution limit [Å] | 2.100 * | 2.100 * |
Rmerge | 0.080 | 0.190 * |
Total number of observations | 27125 * | |
Number of reflections | 6988 | |
Completeness [%] | 85.2 | 66.4 * |
Redundancy | 3.88 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, sitting drop * | 6.5 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 10 (mg/ml) | |
2 | 1 | reservoir | PEG8000 | 18 (%) | |
3 | 1 | reservoir | zinc acetate | 0.2 (M) | |
4 | 1 | reservoir | sodium cacodylate | 0.1 (M) |