1CPM

NATIVE-LIKE IN VIVO FOLDING OF A CIRCULARLY PERMUTED JELLYROLL PROTEIN SHOWN BY CRYSTAL STRUCTURE ANALYSIS

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	39.430, 44.300, 128.340
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 2.000
R-factor	0.153
Rwork	0.153
RMSD bond length	0.021
RMSD bond angle	2.785
Phasing software	X-PLOR
Refinement software	TNT

Data quality characteristics

	Overall
High resolution limit [Å]	2.000 *
Rmerge	0.033 *
Number of reflections	12507 *
Completeness [%]	85.2 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	7 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	4-morpholineethanesulfonic acid	20 (mM)
2	1	1	EDTA	2 (mM)
3	1	1	CpA16M-59	38 (mg/ml)
4	1	2	PEG4000	12 (%(v/v))
5	1	2	sodium acetate	0.1 (M)
6	1	2		5 (mM)