1CPG
A CATION BINDING MOTIF STABILIZES THE COMPOUND I RADICAL OF CYTOCHROME C PEROXIDASE
Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 105.170, 74.180, 45.220 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.200 |
R-factor | 0.164 |
Rwork | 0.164 |
RMSD bond length | 0.010 |
RMSD bond angle | 2.700 |
Phasing software | X-PLOR |
Refinement software | TNT |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.200 * |
Rmerge | 0.055 * |
Total number of observations | 71833 * |
Number of reflections | 16458 * |
Completeness [%] | 87.1 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, sitting drop * | 6 * | 4 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 10 (mg/ml) | |
2 | 1 | drop | potassium phosphate | 0.10 (M) | |
3 | 1 | drop | MPD | 40 (%(v/v)) | |
4 | 1 | reservoir | MPD | 30 (%(v/v)) |