1COT

X-RAY STRUCTURE OF THE CYTOCHROME C2 ISOLATED FROM PARACOCCUS DENITRIFICANS REFINED TO 1.7 ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	31.600, 42.100, 81.600
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.000 - 1.700
R-factor	0.175
RMSD bond length	0.007
RMSD bond angle	2.260
Refinement software	TNT

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	1.700 *	1.700 *
Rmerge	0.038 *	0.094 *
Total number of observations	37878 *
Number of reflections	12199 *	2078 *
Completeness [%]	97.0 *	92 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	7.5 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	ammonium sulfate	3.3-3.5 (M)
2	1	reservoir	HEPES	50 (mM)